Favourite video game boss fights for me are in The Shadow of the Colossus, very few other games have such good boss fight design.
I'd probably go with Terra's Armor from KH2 FM. The very assence of overpowered superboss, even Sephiroth can't put a finger on him... or rather it.
I thought the Storm King fight in Demon's Souls using the Storm Ruler Sword was effing awesome.
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